| 简介 |
FIELD : organic chemistry, chemical technology.SUBSTANCE : invention relates to the improved method for preparing O, O-dialkyldithiophosphates that are used broadly as flotation agents in concentration of nonferrous, rare and precious metal ores. Invention describes a method for preparing O, O-dialkyldithiophosphates involving preparing O, O-dialkyldithiophosphoric acid by interaction of phosphorus pentasulfide with aliphatic alcohol in solvent medium followed by treatment with alkaline agent. O, O-dialkyldithiophosphoric acid is used as a solvent in the mass ratio of phosphorus pentasulfide and O, O-dialkyldithiophosphoric acid = 1 : 0.2, not less. Invention provides simplifying process, reducing waste in manufacture due to exclusion from technological process the additional using substances as a solvent not taking part in the main reactions, and enhanced yield of the end product.EFFECT : improved preparing method.2 cl, 1 tbl, 11 ex |
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